Performance parameters for analytical method validation: Controversies and discrepancies among numerous guidelines

Analytical Method Validation for Biopharmaceuticals

semi-analytical solution for static and forced vibration problems of laminated beams through smooth fundamental functions method

در این پایان نامه روش جدیدی مبتنی بر روش حل معادلات دیفرانسیل پارهای بر اساس روش توابع پایه برای حل مسایل ارتعاش اجباری واستاتیک تیرها و صفحات لایه ای ارایه شده است که می توان تفاوت این روش با روش های متداول توابع پایه را در استفاده از توابع هموار در ارضاء معادلات حاکم و شرایط مرزی دانست. در روش ارایه شده در این پایاننامه از معادله تعادل به عنوان معادله حاکم بر رفتار سیستم استفاده شده است که مو...

Tributyltin in Crustacean Tissues: Analytical Performance and Validation of Method

O ermitão Clibanarius vittatus é um organismo típico de regiões intertidais estuarinas sendo considerado um possível bioindicador da presença de tributilestanho (TBT) nesses ambientes. Por esta razão, este estudo apresenta o desempenho analítico e a validação do método para quantificação de TBT em tecidos de C. vittatus por cromatografia gasosa com detector fotométrico de chama pulsante (GC-PFP...

Analytical Method Validation

In pharmaceutical industries, the validation of analytical methods is used to demonstrate that the method is fitted for its purpose; it must follow a plan which includes scope, performance characteristics, and acceptance limits. Analytical methods need to be validated or revalidated prior to their introduction into routine analyses (release of batch). The overarching philosophy in current good ...

Development and Validation of a Terbium-Sensitized Luminescence Analytical Method for Deferiprone

A sensitive fluorometric method for the determination of deferiprone (DFP) based on the formation of a luminescent complex with Tb3+ ions in aqueous solutions is reported. The maximum excitation and emission wavelengths were 295 and 545 nm, respectively. The effects of various factors on the luminescence intensity of the system were investigated and optimized, then under the optimum conditions,...